分析化学与检测应用

课程编码：1801010830I0P1008Y 英文名称：Analytical Chemistry and Measurement Application 课时：50 学分：2.50 课程属性：学科核心课 主讲教师：董慧峪等

This course gives an introduction to analytical chemistry and an overview of important analytical methods and their range of application within detection of inorganic and organic compounds. Theory provides the learner with exposure to various laboratory analytical principles used in processing laboratory specimens and the application of theory with selected laboratory procedures. The learner will study spectrophotometry, reflectance photometry, chromatography, osmometry, electrophoresis, immunochemistry, general electricity, electrodes and basic automation.

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第一章 Introduction 3学时 董慧峪
第1节 Classification of Analytical Methods
第2节 Types of Instrumental Methods
第3节 Instruments for Analysis
第4节 Calibration of Instrumental Methods
第5节 Selecting an Analytical Method
第二章 Measurement Basics 2学时 董慧峪
第1节 Electrical Components and Circuits
第2节 Operational Amplifiers in Chemical
第3节 Digital Electronics and Computers
第4节 Signals and Noise
第三章 Introduction to Spectrometric Methods 1学时 董慧峪
第1节 General Properties of Electromagnetic Radiation
第2节 Wave Properties of Electromagnetic Radiation
第3节 Quantum-Mechanical Properties of Radiation
第4节 Quantitative Aspects of Spectrochemical Measurements
第四章 Components of Optical Instruments and Optical Atomic Spectrometry 3学时 董慧峪
第1节 General Designs of Optical Instruments
第2节 Sources of Radiation
第3节 Wavelength Selectors and Sample Containers
第4节 Radiation Transducers
第5节 Signal Processors and Readouts
第6节 Fiber Optics
第7节 Types of Optical Instruments
第8节 Optical Atomic Spectra
第9节 Atomization Methods
第10节 Sample-Introduction Methods
第五章 Atomic Absorption, Atomic Fluorescence Spectrometry and Atomic Emission Spectrometry 2学时 董慧峪
第1节 Sample Atomization Techniques
第2节 Atomic Absorption Instrumentation
第3节 Interferences in Atomic Absorption Spectroscopy
第4节 Atomic Absorption Analytical Techniques
第5节 Atomic Fluorescence Spectroscopy
第6节 Emission Spectroscopy Based on Plasma Sources
第7节 Emission Spectroscopy Based on Arc and Spark Sources
第8节 Other Sources for Optical Emission Spectroscopy
第六章 Atomic Mass Spectrometry and Atomic X-ray Spectrometry 2学时 董慧峪
第1节 Some General Features of Atomic Mass Spectrometry
第2节 Mass Spectrometers
第3节 Inductively Coupled Plasma Mass Spectrometry
第4节 Spark Source Mass Spectrometry
第5节 Glow-Discharge Mass Spectrometry
第6节 Other Mass Spectrometric Methods
第7节 Fundamental Principles
第8节 Instrument Components
第9节 X-ray Fluorescence Methods and X-ray Absorption Methods
第10节 The Electron Microprobe
第七章 Applications of Ultraviolet-Visible Molecular 2学时 董慧峪
第1节 Measurement of Transmittance and Absorbance
第2节 Beer’s Law
第3节 The Effects of Instrumental Noise on Spectrophotometric Analyses
第4节 Magnitude of Molar Absorptivities
第5节 Absorbing Species
第6节 Qualitative Applications of Ultraviolet Visible Absorption Spectroscopy
第7节 Quantitative Analysis by Absorption Measurements
第8节 Photometric and Spectrophotometric Titrations
第9节 Spectrophotometric Kinetic Methods
第10节 Spectrophotometric Studies of Complex Ions
第八章 Molecular Luminescence Spectrometry 1学时 董慧峪
第1节 Theory of Fluorescence and Phosphorescence
第2节 Fluorescence and Phosphorescene Instrumentation
第3节 Applications of Photoluminescence Methods
第4节 Chemiluminescence
第九章 Applications of Infrared Spectrometry 2学时 董慧峪
第1节 Theory of IR Absorption Spectrometry
第2节 IR Instrumentation
第3节 IR Sources and Transducers
第4节 Mid-IR Absorption Spectrometry
第5节 Mid-IR Reflection Spectrometry
第6节 Photoacoustic IR Spectroscopy
第7节 Near-IR and Far-IR Spectroscopy
第8节 IR Emission Spectroscopy
第9节 IR Microscopy and Imaging
第十章 Raman Spectroscopy and Nuclear Magnetic Resonance Spectroscopy 2学时 董慧峪
第1节 Theory of Raman Spectroscopy
第2节 Instrumentation
第3节 Applications of Raman Spectroscopy
第4节 Other Types of Raman Spectroscopy
第5节 Theory of NMR
第6节 Environmental Effects on NMR Spectra
第7节 NMR Spectrometers
第8节 Applications of Proton NMR
第9节 Carbon-13 NMR
第10节 Magnetic Resonance Imaging
第十一章 Molecular Mass Spectrometry 3学时 贲伟伟
第1节 Molecular Mass Spectra
第2节 Ion Sources
第3节 Mass Spectrometers
第4节 Applications of Molecular Mass Spectrometry
第5节 Quantitative Applications of Mass Spectrometry
第十二章 An Introduction to Chromatographic Separations 3学时 贲伟伟
第1节 General Description of Chromatography
第2节 Migration Rates of Solutes
第3节 Band Broadening and Column
第4节 Optimization of Column
第5节 Summary of Chromatographic Relationships
第6节 Applications of Chromatography
第十三章 Gas Chromatography 3学时 贲伟伟
第1节 Principles of GLC
第2节 Instruments for GLC
第3节 Gas Chromatographic Columns and Stationary Phases
第4节 Applications of GC
第5节 Advances in GC
第6节 Gas-Solid Chromatography
第十四章 High-Performance Liquid Chromatography 3学时 贲伟伟
第1节 Scope of HPLC
第2节 Column Efficiency in LC
第3节 Instrumentation
第4节 Partition Chromatography
第5节 Adsorption Chromatography
第6节 Ion Chromatography
第7节 Size-Exclusion Chromatography
第8节 Affinity Chromatography
第9节 Thin-Layer Chromatography
第十五章 Electroanalytical Chemistry 4学时 贲伟伟
第1节 Electrochemical Cells
第2节 Potentials in Electroanalytical Cells
第3节 Electrode Potentials
第4节 Calculation of Cell Potentials from Electrode Potentials
第5节 Currents in Electrochemical Cells
第6节 Types of Electroanalytical Methods
第十六章 Surface Characterization by Spectroscopy and Microscopy 4学时 贲伟伟
第1节 Introduction to the Study of Surfaces
第2节 Spectroscopic Surface Methods
第3节 Electron Spectroscopy
第4节 Ion Spectroscopic Techniques
第5节 Surface Photon Spectroscopic Methods
第6节 Electron-Stimulated Microanalysis Methods
第7节 Scanning Probe Microscopes
第十七章 Laboratory Portion of Instrumental Analysis I: Determination of Chlorophyll in Olive Oil by UV-Visible and Fluorescence Spectroscopies 3学时 董慧峪
第1节 Measure and analyze the visible light absorbance spectra of three standard olive oils: extra
第2节 Measure the absorbance spectrum of an “unknown” olive oil sample
第3节 Identify the unknown olive oil as one of the three standard types
第4节 Compare the results with those obtained via fluorescence spectroscopy
第十八章 Laboratory Portion of Instrumental Analysis II: Qualitative Gas Chromatography: The Van Deemter plot and optimum separation 3学时 董慧峪
第1节 Effect of column gas flow rate on isothermal GC separation of BTEX compounds
第2节 Effect of column temperature and temperature programming
第3节 Quantitative analysis of BTEX-components in a gasoline sample
第十九章 Laboratory Portion of Instrumental Analysis III: "Imposter" vs. "Real" Perfumes via GC-MS 2学时 董慧峪
第1节 Tuning the instrument
第2节 Setting up a method
第3节 Running a Method
第4节 Data Analysis
第二十章 Final Presentation 3学时 董慧峪
第1节 Final presentation

Dr. Huiyu Dong obtained his B.Sc. and Master's degree from Department of Environmental Engineering, Tianjin University in 2006 and 2008, respectively. He then obtained his Ph.D. degree at Research Center for Eco-environmental Sciences (RCEES), Chinese Academy of Sciences in 2012. In 2012, he joined RCEES as an Assistant Professor and was promoted to Associate Professor in 2019. At RCEES, he continued his research into controlling water pollution with an emphasis on disinfection by-products, micro-pollutants and advanced treatment processes for safe supply of drinking water. He worked at the University of Barcelona and Swiss federal Institute of Technology in Lausanne (EPFL) with Marie Sk?odowska-Curie Actions in 2015. In 2018-2019, he began research as a visiting scholar in Susan Richardson’s group, University of South Carolina. He has published more than 90 SCI research papers including Accounts Chem. Res., Environ. Sci. Technol., Water Res., Chem. Eng. J., and J. Hazard. Mater.